Development and Scale-Up of a Key Copper-Catalyzed Biaryl Ether Formation for the Multikilogram Synthesis of Emprumapimod

Christopher Brearley, Robert David Bright, James Clarke,Douglas J. Critcher,Susana Torres, Ingrid Edwards,Harriet Fenton, Shanjun Huang, Rebecca Amy Johnson, Ricky A. Jones, Suju P. Mathew, Rhys Norster, Kathryn Alice Starbuck, Amelia Taylor-Young,William Waddington,Robert Walton, Jimmy Wang

Organic Process Research & Development（2024）

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ullmann-type coupling,process development,nonprecious metal catalysis,copper catalysis,biaryl etherification

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