Water-soluble Titanium-Polyoxomolybdate with External Μ3 Bridging Oxygen Coordination on a Lacunary Keggin Structure.
Chemical Communications（2019）
Northeast Normal Univ
Abstract
A titanium-polyoxomolybdate K6(H3O)8[{PMo9O34TiO}2]·32H2O (1) was successfully synthesized and structurally characterized. It is an unprecedented instance that the titanium-containing polyoxomolybdate is water-soluble and was synthesized by using a conventional aqueous solution method. The Ti4+ ions exist in an unusual coordination mode. Besides, compound 1 as a wide band gap semiconductor showed evident photocatalytic activity for the oxidation of benzaldehyde into benzoic acid.
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